Solid State and Crystallization

 
The Curious Case of Acetaldehyde Phenylhydrazone: Resolution of a 120 Year Old Puzzle Where Forms With Vastly Different Melting Points Have the Same Structure
C.E.S. Bernardes, M. Carravetta, S.J. Coles, E.R.H. van Eck, H. Meekes, M.E. Minas da Piedade, M.B. Pitak, M. Podmore, T. Ruiter, L. Sögütoglu, R.R.E. Steendam, T.L. Threlfall
Crystal Growth & Design 2019, ASAP.
DOI:10.1021/acs.cgd.8b01459

Polymorphism in Simvastatin: Twinning, Disorder and Enantiotropic Phase Transitions
R.G. Simões, C.E.S. Bernardes, A. Joseph, M.F.M. Piedade, W. Kraus, F. Emmerling, H.P. Diogo, M.E. Minas da Piedade
Molecular Pharmaceuticals 2018, 15, 5349-5360.
DOI:10.1021/acs.molpharmaceut.8b00818

A New Polymorph of 1-(4-Hydroxyphenyl)pentan-1-one Revealed by Thermoanalytical and X-ray Diffraction Studies
C.S.D. Lopes, C.E.S. Bernardes, M.F.M. Piedade, H.P. Diogo, M.E. Minas da Piedade
The European Physical Journal Special Topics 2017, 226, 849-855.
DOI:10.1140/epjst/e2016-60187-0

Polymorphic Phase Transition in 4’-Hydroxyacetophenone: Equilibrium Temperature, Kinetic Barrier and the Relative Stability of Z’ = 1 and Z’ = 2 Forms
A. Joseph, C.E.S. Bernardes, A.I. Druzhinina, R.M. Varushchenko, T.Y. Nguyen, F. Emmerling, L. Yuan, V. Dupray, G. Coquerel, M.E. Minas da Piedade
Crystal Growth & Design 2017, 17, 1918-1932.
DOI:10.1021/acs.cgd.6b01876

A New Polymorph of 1-(4-Hydroxyphenyl)pentan-1-one Revealed by Thermoanalytical and X-ray diffraction Studies
C.S.D. Lopes, C.E.S. Bernardes, M.F.M. Piedade, H.P. Diogo, M.E. Minas da Piedade
European Physics Journal Special Topics 2017, 226, 849–855.
DOI:10.1140/epjst/e2016-60187-0

Kinetics and Mechanism of the Thermal Dehydration of a Robust and Yet Metastable Hemihydrate of 4-Hydroxynicotinic Acid.
A. Joseph, C.E.S. Bernardes, A.S. Viana, M.F.M. Piedade, M.E. Minas da Piedade
Crystal Growth and Design 2015, 15, 3511-3524.
DOI:10.1021/acs.cgd.5b00594

Size Matters: An Experimental and Computational Study of the Influence of Particle Size on the Lattice Energy of NaCl.
S. Range, C. E. S. Bernardes, R. G. Simões, M. Epple, M. E. Minas da Piedade
Journal of Physical Chemistry C 2015, 119, 4387-4396.
DOI:10.1021/jp5124772

From Molecules to Crystals: The Solvent Plays an Active Role Throughout the Nucleation Pathway of Molecular Organic Crystals.
C. E. S. Bernardes, M. L. S. Matos Lopes, J. R. Ascenso, M. E. Minas da Piedade
Crystal Growth and Design 2014, 14, 5436-5441.
DOI:10.1021/cg500609g

Thermal Stability of Simvastatin under Different Atmospheres.
R. G. Simões, H. P. Diogo, A. Dias, M. C. Oliveira, C. Cordeiro, C. E. S. Bernardes, M. E. Minas da Piedade
Journal of Pharmaceutical Sciences 2014, 103, 241-248.
DOI:10.1002/jps.23787

Polymorphism in 4'-Hydroxyacetophenone: A Vibrational Analysis.
C. E. S. Bernardes, L. M. Ilharco, M. E. Minas da Piedade
Journal of Molecular Structure 2014.
DOI:10.1016/j.molstruc.2013.11.050

Energetics and Structure of Simvastatin.
R. G. Simões, C. E. S. Bernardes, H. P. Diogo, F. Agapito, M. E. Minas da Piedade
Molecular Pharmaceutics 2013 10, 2713-2722.
DOI:10.1021/mp400132r

Polymorphism in 4-Hydroxybenzaldehyde: A Crystal Packing and Thermodynamic Study.
R. G. Simões, C. E. S. Bernardes, M. E. Minas da Piedade
Crystal Growth and Design 2013 13, 2803-281.
DOI:10.1021/cg400123p

Crystallization of 4'-Hydroxyacetophenone from Water: Control of Polymorphism via Phase Diagram Studies
C. E. S. Bernardes, M. E. Minas da Piedade
Crystal Growth and Design 2012, 12, 2932-2941.
DOI:10.1021/cg300134z

Solubility of Nicotinic Acid in Water, Ethanol, Acetone, Diethyl Ether, Acetonitrile, and Dimethyl Sulfoxide
E. M. Gonçalves, M. E. Minas da Piedade
Journal Chemical Thermodynamics 2012, 47, 362-371.
DOI:10.1016/j.jct.2011.11.023

Polymorphism in 4'-Hydroxyacetophenone: A Molecular Dynamics Simulation Study
C. E. S. Bernardes, M. E. Minas da Piedade, J. N. Canongia Lopes
Journal of Physical Chemistry B 2012, 116, 5179-5184.
DOI:10.1021/jp300341f

Heat Capacity and Thermodynamics of Solid and Liquid Pyridine-3-carboxylic Acid (Nicotinic Acid) Over the Temperature Range 296 K to 531 K
A. Joseph, C. E. S. Bernardes, M. E. Minas da Piedade
Journal Chemical Thermodynamics 2012, 55, 23-28.
DOI:10.1016/j.jct.2012.06.010

Thermodynamic Characterization of Three Polymorphic Forms of Piracetam
R. Picciochi, H. P. Diogo, M. E. Minas da Piedade
Journal of Pharmaceutical Sciences 2011, 100, 594-603.
DOI:10.1002/jps.22294

A Robust Yet Metastable New Hemihydrate of 4-Hydroxynicotininc Acid
E. P. Matias, C. E. S. Bernardes,a, M. F. M. Piedade, M. E. Minas da Piedade
Crystal Growth & Design 2011, (ASAP).
DOI:10.1021/cg1015687

Thermodynamic Characterization of Three Polymorphic Forms of Piracetam
R. Picciochi, H. P. Diogo, M. E. Minas da Piedade
Journal of Pharmaceutical Sciences 2010, 100, 594-603.
DOI:10.1002/jps.22294

Structure and Energetics of a New Hydrate of 4'-Hydroxyacetophenone
C. E. S. Bernardes, M. F. M. Piedade, M. E. Minas da Piedade
Crystal Growth & Design 2010, 10, 2419-2430.
DOI:10.1021/cg7012792

Thermochemistry of Paracetamol
R. Picciochi, H. P. Diogo, M. E. Minas da Piedade
Journal of Thermal Analysis and Calorimetry 2010, 100, 391-401.
DOI:10.1007/s10973-009-0634-y

Polymorphism in 4'-Hydroxyacetophenone: Structure and Energetics
C. E. S. Bernardes, M. F. M. Piedade, M. E. Minas da Piedade
Crystal Growth & Design 2008, 8, 2419-2430.
DOI:10.1021/cg7012792